4-甲氧基-N,N-二甲基-苯甲酰胺合成路线 （共 45 条）
反应条件
cesium fluoride; copper
T=180°C; 4 h;
参考文献
Langlois, Bernard R.; Roques, Nicolas
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1318 - 1325
反应条件
amination; 12 h; Heating;
参考文献
Woo Song Lee; Ki Hun Park; Yoon
Synthetic Communications, 2000 , vol. 30, # 23 p. 4241 - 4245
反应条件
hydrogenchloride
Yield given;
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
1: 1.) lithium diisopropylamide / 2.) 5 h
2: 2n HCl
View Scheme
参考文献
Boche, Gernot; Bosold, Ferdinand; Niessner, Manfred
Tetrahedron Letters, 1982 , vol. 23, # 32 p. 3255 - 3256
反应条件
sodium methylate in methanol
T=25°C; 3480 h; Equilibrium constant;
参考文献
Guthrie, J. Peter; Pike, David C.; Lee, Yiu-Chung
Canadian Journal of Chemistry, 1992 , vol. 70, # 6 p. 1671 - 1683
反应条件
tetrabutylammomium bromide; Ni(2,2'-bipyridyl)(carbon monoxide)2 in various solvent(s)
Ambient temperatureelectrolysis, -1.6 V; Product distributionMechanism;
参考文献
Garnier, L.; Rollin, Y.; Perichon, J.
Journal of Organometallic Chemistry, 1989 , vol. 367, p. 347 - 358
反应条件
in chloroform-d1
T=70°C; k = 4.1E-6/sec; Rate constant;
参考文献
Symes, Jill; Modro, Tomasz A.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1702 - 1708
反应条件
1: 2.) n-BuLi / 1.) benzene, room temp., 4 h 2.) THF, -20 deg C, 24 h
2: 2.) H2O, H(1+) / 1.) THF, -42 deg C
View Scheme
参考文献
Comins, Daniel L.; Brown, Jack D.
Tetrahedron Letters, 1983 , vol. 24, # 49 p. 5465 - 5468
反应条件
(i) EtBr, Mg, THF, (ii) /BRN= 389219/; Multistep reaction;
参考文献
Somin,I.N.; Germanguz,E.A.
Journal of Organic Chemistry USSR (English Translation), 1969 , vol. 5, p. 1727 - 1730
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 1780 - 1783
反应条件
HPtCl6·6H2O; 1,1,3,3-tetramethyldisiloxane in tetrahydrofuran; toluene
T=75°C; 5 h; Inert atmosphere; chemoselective reaction;
参考文献
Tsutsumi, Hironori; Sunada, Yusuke; Nagashima, Hideo
Chemical Communications, 2011 , vol. 47, # 23 p. 6581 - 6583
