2-甲氧基-N,N-二甲基-苯甲酰胺合成路线 （共 13 条）
反应条件
Yield given. Multistep reaction;
参考文献
Iwao, Masatomo; Kuraishi, Tsukasa
Tetrahedron Letters, 1985 , vol. 26, # 50 p. 6213 - 6216
反应条件
zirconocene dichloride; lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=20°C; 0.0333333 h;
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
反应条件
(i) EtBr, Mg, THF, (ii) /BRN= 2088722/; Multistep reaction;
参考文献
Somin,I.N.; Germanguz,E.A.
Journal of Organic Chemistry USSR (English Translation), 1969 , vol. 5, p. 1727 - 1730
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 1780 - 1783
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water
T=90°C; 12 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
sodium methylate; nickel diacetate in 1,4-dioxane
T=110°C;
参考文献
Ju, Jinhun; Jeong, Miso; Moon, Jeongju; Hyun, Min Jung; Lee, Sunwoo
Organic Letters, 2007 , vol. 9, # 22 p. 4615 - 4618
参考文献
Brown,H.C.; Tsukamoto,A.
Journal of the American Chemical Society, 1964 , vol. 86, p. 1089 - 1095
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water
T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
1,1'-carbonyldiimidazole
T=160 - 165°C; 1 h;
参考文献
Aavula, Sanjeev Kumar; Chikkulapally, Anil; Hanumanthappa; Jyothi, Indira; Vinod; Sulur, Kumar; Manjunatha; Sythana, Suresh Kumar
Journal of Chemical Research, 2013 , vol. 37, # 3 p. 155 - 159
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate
T=135°C; 6 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / toluene / 20 °C
2: triethylamine / dichloromethane / 0 - 20 °C
View Scheme
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
