4,4'-二叔丁基-2,2'-联吡啶合成路线 （共 9 条）
反应条件
manganese; nickel(II) bromide trihydrate in N,N-dimethyl-formamide T=20 - 60°C; 20 h; Inert atmosphere;
参考文献
Synthesis (Germany), , vol. 45, # 22 art. no. SS-2013-M0415-PSP, p. 3099 - 3102
反应条件
nickel in neat (no solvent) 10 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 63, # 6 p. 1675 - 1702
反应条件
1: acetonitrile / -35 - 20 °C / Inert atmosphere 2: Na[HB(OMe)3] / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
1: water; sodium hydroxide / 1.5 h / 100 °C / Inert atmosphere 2: acetonitrile / -35 - 20 °C / Inert atmosphere 3: Na[HB(OMe)3] / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
1: acetonitrile / -35 - 20 °C / Inert atmosphere 2: sodium tetrahydroborate / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
1: water; sodium hydroxide / 1.5 h / 100 °C / Inert atmosphere 2: acetonitrile / -35 - 20 °C / Inert atmosphere 3: sodium tetrahydroborate / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
1: acetonitrile / -35 - 20 °C / Inert atmosphere 2: sodium tetrahydroborate / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
1: water; sodium hydroxide / 1.5 h / 100 °C / Inert atmosphere 2: acetonitrile / -35 - 20 °C / Inert atmosphere 3: sodium tetrahydroborate / acetonitrile / Inert atmosphere View Scheme
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 65, # 7 p. 861 - 872
反应条件
in benzene-d6 Inert atmosphere;
参考文献
Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip
Organometallics, 2013 , vol. 32, # 10 p. 3091 - 3107
