2-甲氧基-6-甲基-3-吡啶甲醛合成路线 (共 2 条)
反应条件
1: 83 percent / CH2Cl2 / 48 h / Ambient temperature
2: 1.) Diisobutylaluminium hydride, 2.) 10percent aq. KOH / 1.) Toluene, -78 deg C, 30 min, 2.) RT, 3 h
View Scheme
参考文献
Beak, Peter; Covington, Johnny B.; Smith, Stanley G.; White, J. Matthew; Zeigler, John M.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1354 - 1362
反应条件
potassium hydroxide; diisobutylaluminium hydride
1.) Toluene, -78 deg C, 30 min, 2.) RT, 3 h; Yield given. Multistep reaction;
参考文献
Beak, Peter; Covington, Johnny B.; Smith, Stanley G.; White, J. Matthew; Zeigler, John M.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1354 - 1362