2-甲氧基-6-甲基吡啶-3-羧酸合成路线 (共 3 条)
反应条件
potassium hydroxide in water
3 h; Heating;
参考文献
Beak, Peter; Covington, Johnny B.; Smith, Stanley G.; White, J. Matthew; Zeigler, John M.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1354 - 1362
反应条件
1: 78 percent / aq. NaOH, 30percent H2O2 / aq. ethanol / 3 h / 55 °C
2: 75 percent / aq. KOH (10percent) / H2O / 3 h / Heating
View Scheme
参考文献
Beak, Peter; Covington, Johnny B.; Smith, Stanley G.; White, J. Matthew; Zeigler, John M.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1354 - 1362
反应条件
1: 83 percent / CH2Cl2 / 48 h / Ambient temperature
2: 78 percent / aq. NaOH, 30percent H2O2 / aq. ethanol / 3 h / 55 °C
3: 75 percent / aq. KOH (10percent) / H2O / 3 h / Heating
View Scheme
参考文献
Beak, Peter; Covington, Johnny B.; Smith, Stanley G.; White, J. Matthew; Zeigler, John M.
Journal of Organic Chemistry, 1980 , vol. 45, # 8 p. 1354 - 1362