反式-4-(4-戊基环己基)苯甲酸对氰基苯酚酯合成路线 (共 11 条)
反应条件
1: hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / or in 1:1 mixture of triethanolamine and glycerol 2: AlCl3 / 1,2-dichloro-ethane / 0.5 h 3: aq. NaOH, Br2 / dioxane / 3 h / 35 - 40 °C 4: SOCl2 / 1 h / Heating 5: 69 percent / pyridine / dimethyl ether / overnight View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, p. 1479 - 1483
Zhurnal Organicheskoi Khimii, , vol. 19, # 8 p. 1669 - 1674