反应条件
1: 0.41 g / acetic acid / 26 h / 80 °C 2: 1.) N-methylmorpholine N-oxide, osmium tetroxide; 2.) p-toluenesulfonic acid / 1.) t-butyl alcoho-THF-water (10.10:1), r.t., 18 h; 2.) CHCl3, r.t., 1 h 3: trifluoroperacetic acid, Na2HPO4 (powdered) / CH2Cl2 / 1.) 5 deg C, 1 h; 2.) 30 deg C, 3 h 4: 1.79 g / 10 N NaOH / methanol / 3 h / Heating View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 51, # 7 p. 1909 - 1914
