alpha,alpha-二甲基-4-亚甲基环己烷甲醇合成路线 （共 14 条）
参考文献
Vig,O.P. et al.
Journal of the Indian Chemical Society, 1967 , vol. 44, # 5 p. 388 - 390
反应条件
trichlorophosphate in pyridine
15 h; Yield given. Yields of byproduct given;
参考文献
Brecknell, Douglas J.; Carman, Raymond M.; Edwards, Ross A.; Hansford, Karl A.; Karoli, Tomislav; Robinson, Ward T.
Australian Journal of Chemistry, 1997 , vol. 50, # 7 p. 689 - 700
反应条件
1: 82 mg / N-bromosuccinimide / acetone; H2O / 1 h / Ambient temperature
2: NaOH / methanol / 0.08 h
3: p-TsOH / CH2Cl2 / 2 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
反应条件
1: 1.1 g / KMnO4, KOH / H2O; 2-methyl-propan-2-ol / 0.5 h
2: 630 mg / pyridine / 2 °C
3: LiAlH4 / diethyl ether / 1 h
View Scheme
参考文献
Bull, Steven D.; Carman, Raymond M.
Australian Journal of Chemistry, 1993 , vol. 46, # 12 p. 1869 - 1880
