反应条件
1: 79 percent / LiAlH4 / tetrahydrofuran / 16 h / Ambient temperature 2: pyridine / 16 h / Ambient temperature 3: 1.) acetyl bromide, 30 percent hydrobromide / 1.) AcOH, 20 min, r.t.; 2.) toluene, xylene, reflux, 30 min 4: 94 percent / NaOMe / methanol / 1 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 40, # 1 p. 145 - 152
