5-十一烷基二氢-2(3H)-呋喃酮合成路线 (共 5 条)
反应条件
silver trifluoromethanesulfonate in chlorobenzene
T=130°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Goossen, Lukas J.; Ohlmann, Dominik M.; Dierker, Markus
Green Chemistry, 2010 , vol. 12, # 2 p. 197 - 200
反应条件
sodium hydroxide; sodium tetrahydroborate in ethanol
3 h; Ambient temperature;
参考文献
Granata, Alessandro; Perlin, Arthur S.
Canadian Journal of Chemistry, 1993 , vol. 71, # 6 p. 864 - 871
反应条件
samarium diiodide in tetrahydrofuran; tert-butyl alcohol
5 h;
参考文献
Schlutt, Birgit; Moran, Noelia; Schieberle, Peter; Hofmann, Thomas
Journal of Agricultural and Food Chemistry, 2007 , vol. 55, # 23 p. 9634 - 9645
反应条件
1: 1.) cadmium chloride / 1.) diethyl ether, reflux, 45 min, 2.) diethyl ether, reflux, 4 h
2: 72.5 percent / NaBH4, 1 N aq. NaOH / ethanol / 3 h / Ambient temperature
View Scheme
参考文献
Granata, Alessandro; Perlin, Arthur S.
Canadian Journal of Chemistry, 1993 , vol. 71, # 6 p. 864 - 871
参考文献
Delaby; Lecomte
Bulletin de la Societe Chimique de France, 1937 , vol. 4, p. 1007,1011