5,7-二甲基-2,3-二氢-1H-[1,4]二氮杂卓高氯酸盐合成路线 (共 2 条)
反应条件
EDA*2HClO4 in chloroform
Heating;
参考文献
Burgart, Ya. V.; Skryabina, Z. E.; Saloutin, V. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 9.2 p. 1849 - 1853
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 9 p. 2088 - 2092
反应条件
diazoacetic acid ethyl ester
T=100 - 120°C; 10 h; other fluoroalkyl-containing 1,3-dicarbonyl compounds;
参考文献
Skryabina, Z. E.; Burgart, Ya. V.; Saloutin, V. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 4.2 p. 788 - 794
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 4 p. 890 - 896