γ-L-谷氨酰基-4-硝基苯胺合成路线 (共 12 条)
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
1: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C 2: hydrogen / Pd/C / methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
1: 98 percent / triethylamine / methanol / 3 h 2: 90 percent / toluenesulfonic acid / toluene / 3 h / Heating 3: thionyl chloride / CH2Cl2 / 0.5 h / Heating 4: pyridine / CH2Cl2 / 0.25 h / 20 °C 5: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C 6: hydrogen / Pd/C / methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
1: 90 percent / toluenesulfonic acid / toluene / 3 h / Heating 2: thionyl chloride / CH2Cl2 / 0.5 h / Heating 3: pyridine / CH2Cl2 / 0.25 h / 20 °C 4: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C 5: hydrogen / Pd/C / methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
1: pyridine / CH2Cl2 / 0.25 h / 20 °C 2: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C 3: hydrogen / Pd/C / methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
1: thionyl chloride / CH2Cl2 / 0.5 h / Heating 2: pyridine / CH2Cl2 / 0.25 h / 20 °C 3: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C 4: hydrogen / Pd/C / methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 4 p. 1111 - 1118
反应条件
γ-glutamyltransferase from Bacillus subtilis in aq. phosphate buffer T=22°C; pH=8.5; Enzymatic reaction; pH-value;
参考文献
Morelli, Carlo F.; Calvio, Cinzia; Biagiotti, Marco; Speranza, Giovanna
FEBS Journal, 2014 , vol. 281, # 1 p. 232 - 245
反应条件
T=37°C; 0.1 M Tris-HCl buffer, γ-glutamyltransferase from mushroom Lentinus edodes; other enzyme; Michaelis constant Km and Vmax determination;
参考文献
Sharma, Anurag; Kumari, Moni; Jagannadham
Process Biochemistry, 2012 , vol. 47, # 6 p. 914 - 921
反应条件
marine bivalve lysozyme; MOPS buffer; Tapes japonica T=37°C; pH=7.0; Enzyme kinetics;
参考文献
Castellano; Merlino, Antonello; Rossi, Mose; La Cara, Francesco
Biochimie, 2010 , vol. 92, # 5 p. 464 - 474
反应条件
Tris-HCl buffer T=37°C; pH=8.0; Enzyme kinetics; Further Variations:Catalysts;
参考文献
Nakano, Yoshihiro; Okawa, Satoshi; Yamauchi, Takayoshi; Koizumi, Yukio; Sekiya, Jiro
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 2 p. 369 - 376