5,5-二甲己烷2,4-二酮合成路线 （共 27 条）
反应条件
dihydrogen peroxide in water T=25°C; 8 h; Green chemistry;
参考文献
Sun, Xi; Wang, Min; Li, Pinhua; Zhang, Xiuli; Wang, Lei
Green Chemistry, 2013 , vol. 15, # 12 p. 3289 - 3294
反应条件
1: NH2NH2*H2O
2: Cu(OAc)2 / pyridine
View Scheme
参考文献
Mukherjee, Anuradha; Subramanyam; Puranik, Vedavati G.; Mohandas, Thekke P.; Sarkar, Amitabha
European Journal of Inorganic Chemistry, 2005 , # 7 p. 1254 - 1263
参考文献
Escale,R. et al.
Bulletin de la Societe Chimique de France, 1974 , p. 725 - 733
反应条件
T=24°C; Equilibrium constant;
参考文献
Koshimura,H. et al.
Bulletin of the Chemical Society of Japan, 1973 , vol. 46, p. 632 - 634
反应条件
1: 74 percent / 1.) NaH / benzene / 1.) 10 deg C, 1 h, room temperature, 2 h, 2.) 6 h
2: copper(II) sulfate / cyclohexane / 14 h / Heating
3: 2 M HCl / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Saigo, Kazuhiko; Kurihara, Hiroshi; Miura, Hisao; Hongu, Akinori; Kubota, Naomi; et al.
Synthetic Communications, 1984 , vol. 14, # 9 p. 787 - 796
反应条件
1: 74 percent / 1.) NaH / benzene / 1.) 10 deg C, 1 h, room temperature, 2 h, 2.) 6 h
2: copper(II) sulfate / cyclohexane / 14 h / Heating
3: 2 M HCl / diethyl ether / 12 h / Ambient temperature
View Scheme
参考文献
Saigo, Kazuhiko; Kurihara, Hiroshi; Miura, Hisao; Hongu, Akinori; Kubota, Naomi; et al.
Synthetic Communications, 1984 , vol. 14, # 9 p. 787 - 796
反应条件
hydrogenchloride; hydroxylamine; sodium acetate
参考文献
Iimura
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 1846,1847
Chem.Abstr., 1959 , p. 2779
