2-(2-甲氧基苯氧基)丙酸合成路线 (共 7 条)
反应条件
2,6-dimethylpyridine; lithium perchlorate in acetonitrile Electrochemical reaction;
参考文献
Journal of Organic Chemistry, , vol. 67, # 13 p. 4458 - 4465
反应条件
1: With water; potassium hydroxide in ethanol
0.75 h; Reflux;
2: With hydrogenchloride in water
参考文献
Carocci, Alessia; Catalano, Alessia; Lovece, Angelo; Lentini, Giovanni; Duranti, Andrea; Lucini, Valeria; Pannacci, Marilou; Scaglione, Francesco; Franchini, Carlo
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 17 p. 6496 - 6511
反应条件
1: KI; K2CO3 / acetone / 22 h / Heating
2: 1.36 g / aq. KOH / ethanol / 24 h / Heating
View Scheme
参考文献
Deffieux, Denis; Fabre, Isabelle; Courseille, Christian; Quideau, Stephane
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4458 - 4465
反应条件
sodium hydroxide in water
20 h; Heating;
参考文献
Segurado, Manuel A. P.; Reis, Joao Carlos R.; De Oliveira, Jaime D. Gomes; Kabilan, Senthamaraikannan; Shanthi, Manohar
Journal of Organic Chemistry, 2007 , vol. 72, # 14 p. 5327 - 5336
反应条件
1: 160 °C
2: potash
View Scheme
参考文献
Bischoff
Chemische Berichte, 1900 , vol. 33, p. 1395
参考文献
Bayer and Co.
Patent: DE261229 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 1105
反应条件
thionyl chloride
T=90°C; 1.5 h;
参考文献
Carocci, Alessia; Catalano, Alessia; Lovece, Angelo; Lentini, Giovanni; Duranti, Andrea; Lucini, Valeria; Pannacci, Marilou; Scaglione, Francesco; Franchini, Carlo
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 17 p. 6496 - 6511