5-(3-甲氧基苯基)-1H-四唑合成路线 （共 5 条）
反应条件
sodium azide; acetic acid in 1-methyl-pyrrolidin-2-one; water T=220°C; P=5250.53 Torr; 0.0833333 h; Microwave irradiation;
参考文献
Gutmann, Bernhard; Roduit, Jean-Paul; Kappe, C. Oliver; Roberge, Dominique
Angewandte Chemie - International Edition, 2010 , vol. 49, # 39 p. 7101 - 7105
反应条件
sodium azide; copper ferrite in N,N-dimethyl-formamide T=120°C; 12 h; Sealed tube;
参考文献
Akula, Ravi Kumar; Adimulam, Chandra S.; Gangaram, Sathaiah; Kengiri, Raju; Banda, Narsaiah; Pamulaparthy, Shanthan R.
Letters in Organic Chemistry, 2014 , vol. 11, # 6 p. 440 - 445
反应条件
1: ammonia; iodine / tetrahydrofuran; water / 1 h / 20 °C 2: sodium azide; iodine / tetrahydrofuran; water / 8.5 h / 100 °C View Scheme
参考文献
Synthetic Communications, , vol. 41, # 14 p. 2081 - 2085
反应条件
1: CuO / N,N-dimethyl-formamide / 100 °C 2: CuO; sodium azide / N,N-dimethyl-formamide View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 35 p. 4732 - 4734
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide 1.) water, methylene dichloride, 25 deg C, 3 h; 2.) 100-120 deg C; Yield given. Multistep reaction;
参考文献
Osipova, T. P.; Koldobskii, G. I.; Ostrovskii, V. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 1018 - 1019
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1119 - 1120
