反应条件
1: 1-Bromo(1H-tetrazol-5-yl)benzene With zinc trifluoromethanesulfonate in acetonitrile 24 h; Heating; 2: [4-(hydroxymethyl)-phenyl]-boronic acid With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in ethylene glycol dimethyl ether; water Suzuki reaction; 24 h; Heatingsolid phase synthesis; 3: With trifluoroacetic acid in dichloromethane 4 h; Further stages.;
参考文献
Cousaert, Nicolas; Willand, Nicolas; Gesquiere, Jean-Claude; Tartar, Andre; Deprez, Benoit; Deprez-Poulain, Rebecca
Tetrahedron Letters, 2008 , vol. 49, # 17 p. 2743 - 2747
