2,6-二甲酰-4-甲基苯酚合成路线 （共 21 条）
反应条件
potassium dichromate; copper diacetate; ethylenediamine 1.) DMSO, r.t., 30 min, 2.) DMSO, 100 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 4 p. 325 - 326
反应条件
trichlorophosphate 1.) 30 deg C, 1 h, 2.) 20-30 deg C, 10 h; boiling water bath, 6h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 8 p. 779 - 781
参考文献
DE580981 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 533
反应条件
in cyclohexane T=22°C; Equilibrium constant;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, , vol. 32, # 1-3 p. 20 - 24
反应条件
in methanol reaction of 2,6-diformyl-4-methylphenol and PTA with Cu(NCS)2 in methanol; filtering off the formed brown solid, concn. of the filtrate to give green crystals as the major component and a small amount of bluish green crystals of the tetranuclear complex;
参考文献
Tandon, Santokh S.; Thompson, Laurence K.; Bridson, John N.; Bubenik, Monica
Inorganic Chemistry, 1993 , vol. 32, p. 4621 - 4631
反应条件
in methanol 1 h; Reflux;
参考文献
Sarkar, Avijit; Ghosh, Aloke Kumar; Bertolasi, Valerio; Ray, Debashis
Dalton Transactions, 2012 , vol. 41, # 6 p. 1889 - 1896
反应条件
toluene-4-sulfonic acid; 2,2-dimethoxy-propane 1 h; Reflux;
参考文献
Hryniewicka, Agnieszka; Morzycki, Jacek W.; Witkowski, Stanislaw
Journal of Organometallic Chemistry, 2010 , vol. 695, # 9 p. 1265 - 1270
反应条件
in methanol 4 h; Heating; Yield given;
参考文献
Adhikary, Bibhutosh; Mandal, Sanat K.; Nag, Kamalaksha
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 935 - 942
反应条件
potassium carbonate in N,N-dimethyl-formamide; acetone
T=20°C; 21 h;
参考文献
Komatsu; Chishiro
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 13 p. 1532 - 1537
反应条件
1: 90 percent / DABCO / dimethylformamide / 15 h / 35 °C
2: 72 percent / BF3*Et2O / toluene / 15 h / 85 °C
View Scheme
参考文献
Brooker, Sally; Croucher, Paul D.; Roxburgh, Fiona M.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 14 p. 3031 - 3037
