3,5-二甲氧基苯甲醛合成路线 （共 226 条）
反应条件
1.1: NaOMe / dimethylformamide / 0 °C 1.2: dimethylformamide / 20 °C 2.1: pyridine hydrochloride / 190 °C View Scheme
参考文献
Ali; Kondo; Tsuda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1130 - 1136
反应条件
copper quinolate; tetra-(n-butyl)ammonium iodide in water; dimethyl sulfoxide T=120°C; 24 h;
参考文献
Zhu, Yan; Yan, Hong; Lu, Linhua; Liu, Defu; Rong, Guangwei; Mao, Jincheng
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9898 - 9905
反应条件
potassium cyanide; potassium iodide T=75 - 80°C; 24 h;
参考文献
Atta, Ananta Kumar; Kim, Seul-Bi; Cho, Dong-Gyu
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 6 p. 2070 - 2072
反应条件
piperidine in pyridine T=110°C; 5 h;
参考文献
Carter, Rachel H.; Garson, Mary J.; Hill, Robert A.; Staunton, James; Sunter, David C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 471 - 479
参考文献
Asahina; Matsuzaki
Yakugaku Zasshi, 1924 , # 509 p. 2
Chem. Zentralbl., 1925 , vol. 96, # I p. 1713
Full Text Show Details
Asahina; Matsuzaki
Chem.Abstr., 1925 , vol. 19, p. 51
反应条件
sodium methylate in N,N-dimethyl-formamide T=20°C; Wittig reaction; 10 h;
参考文献
Free Radical Research, , vol. 45, # 11-12 p. 1379 - 1387
反应条件
1: acetic anhydride; triethylamine 2: copper; quinoline View Scheme
参考文献
Food Chemistry, , vol. 135, # 3 p. 1011 - 1019
反应条件
1: 90 percent / tetrahydrofuran; hexane / 1 h / -78 - 20 °C 2: 74 percent / p-toluenesulfonic acid / toluene / 1 h / Heating 3: 80 percent / H2 / Pd/C / methanol / 20 h / 20 °C View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
(i) Et2O, (ii) H2, Pd-C, AcOEt; Multistep reaction;
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
反应条件
oxygen; copper; ammonium chloride in pyridine T=60°C; 24 h;
参考文献
Capdevielle, Patrice; Lavigne, Andre; Maumy, Michel
Synthesis, 1989 , # 6 p. 451 - 452
