3,5-二甲氧基苯甲醛合成路线 （共 226 条）
反应条件
(i) LiAlH4, (ii) MnO2; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 329 - 331
反应条件
chromium(VI) oxide in acetic acid T=5 - 10°C; 7 h;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 36, # 8 p. 2977 - 2983
反应条件
1: With trifluoroacetic acid in dichloromethane 16 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 1 h;
参考文献
Chemistry - A European Journal, , vol. 11, # 11 p. 3427 - 3442
反应条件
1: 12.7 percent / NaOH / H2O / 2 h / 80 - 90 °C / pH 8.5 - 9 2: 81.8 percent / H2SO4 3: 93.3 percent / N2H4*H2O / 3 h / Heating 4: 75.4 percent / K3[Fe(CN)6]; PEG-400; NH3 / toluene; H2O / 4 h / 10 - 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 41, # 11 p. 2395 - 2398
反应条件
2,6-dimethylpyridine; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; (CuOTf)2*C6H5CH3; oxygen in toluene T=100°C; 42.0833 h; Schlenk techniqueSealed tube; chemoselective reaction;
参考文献
ACS Catalysis, , vol. 3, # 12 p. 3111 - 3122
反应条件
1: 93 percent / Na / tetrahydrofuran / 24 h / Ambient temperature 2: aq. AcOH / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 11 p. 3101 - 3106
反应条件
CpMo(CO)3(CCPh); dihydrogen peroxide in water T=80°C; 8 h; chemoselective reaction;
参考文献
Tetrahedron Letters, , vol. 50, # 24 p. 2885 - 2888
反应条件
1: 27 percent / 1) Na / 1) THF, 24h, r.t., 2) THF, 24h, 0 deg C 2: aq. AcOH / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 11 p. 3101 - 3106
反应条件
1: 80 percent / K / tetrahydrofuran / 24 h / Ambient temperature 2: aq. AcOH / 5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 11 p. 3101 - 3106
反应条件
acetic acid 5 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 57, # 11 p. 3101 - 3106
