3,5-二甲氧基苯甲醛合成路线 （共 226 条）
反应条件
in diethyl ether; N,N-dimethyl-formamide; 1,1-dibromomethane
参考文献
Tanabe Seiyaku Co., Ltd.
Patent: US6048842 A1, 2000 ;
参考文献
Rama Rao; Laxma Reddy; Srinivasa Rao; Vittal; Reddy; Pathi
Tetrahedron Letters, 1996 , vol. 37, # 17 p. 3023 - 3026
反应条件
1: (i) Et2O, (ii) H2, Pd-C, AcOEt
View Scheme
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
反应条件
1: 96 percent / tetrahydrofuran
2: 91 percent / triethylsilane / Pd-C / methanol / 0.08 h
View Scheme
参考文献
Green, Richard H.
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4697 - 4700
反应条件
(i) Et2O, (ii) H2, Pd-C, AcOEt; Multistep reaction;
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
反应条件
1: diethyl ether / 6 h / Heating
2: chromium trioxide / pyridine / 2 h / 0 °C
View Scheme
参考文献
Baylis, Christopher J.; Odle, Stanley W.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 132 - 141
反应条件
ammonium acetate in ethanol
Heating;
参考文献
Muller; Corral; Shire; Wang; Moreira; Kaplan; Stirling
Journal of Medicinal Chemistry, 1996 , vol. 39, # 17 p. 3238 - 3240
反应条件
1: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux
2: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
1: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux
2: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
View Scheme
参考文献
Ayer, William A.; Browne, Lois M.; Lovell, Sarah H.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2267 - 2272
反应条件
(i) Et2O, (ii) H2, Pd-C, AcOEt; Multistep reaction;
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
