2,6-二溴-4-甲基吡啶合成路线 (共 5 条)
反应条件
phosphorus tribromide T=175°C; Substitution; 6 h;
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667
反应条件
1: palladium/strontium carbonate; ethanol / Hydrogenation 2: phosphorus (III)-bromide / 180 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 631,635
反应条件
ammonium hydroxide T=195°C;
参考文献
Bernstein et al.
Journal of the American Chemical Society, 1947 , vol. 69, p. 1147,1148
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=110°C; Substitution; Stille reaction; 16 h;
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene
T=110°C; Substitution; Stille reaction; 16 h;
参考文献
Fallahpour
Synthesis, 2000 , # 12 p. 1665 - 1667