反应条件
1: 1) POCl3, 2) NaOMe / 1) pyridine, r.t., 2) MeOH, r.t., overnight
2: 94 percent / Zn, TiCl4 / tetrahydrofuran; CH2Cl2 / Ambient temperature
3: LiAlH4 / diethyl ether / 3 h
View Scheme
参考文献
Imagawa, Takeshi; Sonobe, Toshihiko; Ishiwari, Hisahiro; Akiyama, Tetsuo; Kawanisi, Mituyosi
Journal of Organic Chemistry, 1980 , vol. 45, p. 2005 - 2006
