2,3-环氧丙基膦酸二乙基酯合成路线 (共 23 条)
反应条件
copper(l) chloride
high β-regioselective nucleophile attack determined by NMR; Product distribution;
参考文献
Nagase, Toshio; Kawashima, Takayuki; Inamoto, Naoki
Chemistry Letters, 1984 , p. 1997 - 2000
反应条件
sodium ethanolate in ethanol
参考文献
Ryabov, B. V.; Ionin, B. I.; Petrov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 5 p. 969 - 983,859 - 871
反应条件
1: 1.) EtONa, 2.) Amberlite H+ / 1.) EtOH, 0 deg C, 1 h,
2: 50 percent / C6H5NH+*ClCrO3- / CH2Cl2 / Ambient temperature
3: 100 percent / diethyldioxirane, Me2CO / 96 h / Ambient temperature
View Scheme
参考文献
Puyau, P. de Macedo; Perie, J. J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1997 , vol. 129, p. 13 - 46