6-溴-6-庚烯-1-基乙酸酯合成路线 (共 3 条)
反应条件
boron tribromide in dichloromethane T=20°C; 5 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 24 p. 6278 - 6281
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 16 h / 0 - 20 °C / |Inert atmosphere 2: boron tribromide / dichloromethane / 5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 24 p. 6278 - 6281
反应条件
1: sodium hydride / 2 h / 20 - 70 °C / |Inert atmosphere 2: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 16 h / 0 - 20 °C / |Inert atmosphere 3: boron tribromide / dichloromethane / 5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 14, # 24 p. 6278 - 6281