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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
73178-23-1
合成路线
（共 10 条）
73178-23-1
→
反应条件
20919-36-2
N-苄基-2-羟基-苯甲酰胺
反应条件
1: With copper(l) iodide; 1,10-phenanthroline; water T=20°C; 0.166667 h; 2: With potassium hydroxide T=100°C; 10 h;
参考文献
Balkrishna, Shah Jaimin; Kumar, Sangit
Synthesis, 2012 , vol. 44, # 9 p. 1417 - 1426
73178-23-1
→
反应条件
2514-36-5
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate; sulfur in N,N-dimethyl-formamide T=110°C; 3 h; Inert atmosphere;
参考文献
Bhakuni, Bhagat Singh; Balkrishna, Shah Jaimin; Kumar, Amit; Kumar, Sangit
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1354 - 1357
73178-23-1
→
反应条件
1684-07-7
3,4-二苯基异苯并吡喃-1-酮
反应条件
1: bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine / toluene / 17 h / 80 °C / Inert atmosphere 2: water; oxalic acid / tetrahydrofuran / 10 h / 60 °C / Inert atmosphere View Scheme
参考文献
Miura, Tomoya; Hiraga, Kentaro; Toyoshima, Takeharu; Yamauchi, Motoshi; Murakami, Masahiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 798 - 800
73178-23-1
+
123-54-6
乙酰丙酮
→
反应条件
29539-21-7
3-甲基异色烯-1-酮
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=100°C; 0.5 h; Inert atmosphere;
参考文献
Kavala, Veerababurao; Wang, Cheng-Chuan; Barange, Deepak Kumar; Kuo, Chun-Wei; Lei, Po-Min; Yao, Ching-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5022 - 5029
673-32-5
1-苯基-1-丙炔
+
73178-23-1
→
反应条件
76836-54-9
反应条件
1: With bis(1,5-cyclooctadiene)nickel (0); potassium carbonate; tris(p-chloro phenyl)phosphine in toluene T=80°C; 17 h; Inert atmosphere; 2: With water; oxalic acid in tetrahydrofuran T=60°C; 10 h; Inert atmosphere;
参考文献
Miura, Tomoya; Hiraga, Kentaro; Toyoshima, Takeharu; Yamauchi, Motoshi; Murakami, Masahiro
Chemistry Letters, 2012 , vol. 41, # 8 p. 798 - 800
73178-23-1
+
88284-48-4
2-(三甲基硅)苯基三氟甲烷磺酸盐
→
反应条件
87861-97-0
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
73178-23-1
→
反应条件
5388-11-4
反应条件
copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide T=80°C; 6 h; Inert atmosphere;
参考文献
Zhou, Jing; Fu, Liangbing; Lv, Man; Liu, Jinsong; Pei, Duanqing; Ding, Ke
Synthesis, 2008 , # 24 art. no. F18308SS, p. 3974 - 3980
73178-23-1
→
反应条件
646029-38-1
反应条件
potassium hexamethylsilazane in toluene T=70 - 80°C; 0.5 h;
参考文献
Marion, Frederic; Coulomb, Julien; Servais, Aurore; Courillon, Christine; Fensterbank, Louis; Malacria, Max
Tetrahedron, 2006 , vol. 62, # 16 p. 3856 - 3871
73178-23-1
+
133816-00-9
→
反应条件
646029-38-1
反应条件
potassium hexamethylsilazane in toluene T=20°C; 24 h;
参考文献
Couty, Sylvain; Liegault, Benoit; Meyer, Christophe; Cossy, Janine
Tetrahedron, 2006 , vol. 62, # 16 p. 3882 - 3895
73178-23-1
→
反应条件
39142-92-2
反应条件
1: 77 percent / bis(triphenylphosphine)palladium(II) chloride; copper(I) iodide; triethylamine / dimethylformamide / 15 h / 80 - 85 °C 2: sodium ethoxide / ethanol / 4 h / Heating 3: hydrogen; glacial acetic acid / Pd-C / 24 h / 20 °C View Scheme
参考文献
Kundu, Nitya G.; Khan, M. Wahab
Tetrahedron, 2000 , vol. 56, # 27 p. 4777 - 4792
