[rhodium(I)chloride(triphenylphosphine)2]1 in acetonitrile-D3; benzene-d6 T=180°C; 1 h; microwave irradiation;
参考文献
Mkhalid, Ibraheem A. I.; Coapes, R. Benjamin; Edes, S. Natasha; Coventry, David N.; Souza, Fabio E. S.; Thomas, Rhodri Ll.; Hall, Jonathan J.; Bi, Si-Wei; Lin, Zhenyang; Marder, Todd B.
Dalton Transactions, 2008 , # 8 p. 1055 - 1064
[rhodium(I)chloride(triphenylphosphine)2]1 in acetonitrile-D3; benzene-d6 T=80°C; 120 h;
参考文献
Mkhalid, Ibraheem A. I.; Coapes, R. Benjamin; Edes, S. Natasha; Coventry, David N.; Souza, Fabio E. S.; Thomas, Rhodri Ll.; Hall, Jonathan J.; Bi, Si-Wei; Lin, Zhenyang; Marder, Todd B.
Dalton Transactions, 2008 , # 8 p. 1055 - 1064
potassium acetate; copper(l) chloride; lithium chloride in N,N-dimethyl-formamide (N2); addn. of DMF and LiCl to CuCl, stirring for 1 h at room temp., addn. of boron compd. and alkyne, stirring at room temp. for 16 h, addn. ofwater; extn. with benzene, washing with water, drying with MgSO4, column chromy(SiO2);
参考文献
Takahashi, Kou; Ishiyama, Tatsuo; Miyaura, Norio
Journal of Organometallic Chemistry, 2001 , vol. 625, # 1 p. 47 - 53
RhCl(CO)(P(C6H5)3)2 in acetonitrile-D3; benzene-d6 (N2); addn. of mixt. of 0.67 equiv. of boron compd. and alkene deriv. tosoln. of 0.03 equiv. of rhodium compd. in 3:1 mixt. of benzene-d6 and a cetonitrile-d3, shaking, heating at 80°C for 5 d; monitoring by NMR and GC-MS;
参考文献
Mkhalid, Ibraheem A. I.; Coapes, R. Benjamin; Edes, S. Natasha; Coventry, David N.; Souza, Fabio E. S.; Thomas, Rhodri Ll.; Hall, Jonathan J.; Bi, Si-Wei; Lin, Zhenyang; Marder, Todd B.
Dalton Transactions, 2008 , # 8 p. 1055 - 1064
