2,4,6-三叔丁基苯酚合成路线 (共 262 条)
反应条件
sulfuric acid; manganese triacetate T=20°C; 3 h; Product distributionMechanism;
参考文献
Batanov, I.A.; Vol'eva, V.B.; Nikiforov, G.A.; Ershov, V.V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 10 p. 2125 - 2130
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 10 p. 2327 - 2332
反应条件
in chloroform; water
参考文献
ICI Americas Inc.
Patent: US4978756 A1, 1990 ;
反应条件
di-tert-butyl peroxide in benzene T=24.84°C; Equilibrium constant;
参考文献
Organic Letters, , vol. 12, # 10 p. 2326 - 2329
反应条件
5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in methanol; dichloromethane T=30°C; oxygen transfer to (TPP)Fe(III)(Cl) with/without buffer; Rate constant;
参考文献
Lee, William A.; Yuan, Lung-Chi; Bruice, Thomas C.
Journal of the American Chemical Society, 1988 , vol. 110, # 13 p. 4277 - 4283
反应条件
1: glacial acetic acid, Br2 / methanol / 0 °C 2: acetic acid / 8 h / 60 - 65 °C 3: 45.6 percent / benzene / 2 h / Irradiation 4: sodium bicarbonate, manganous chloride, O2 / methanol; H2O / 0.75 h 5: 71.3 percent / 1) ceric ammonium nitrate / acetone / 2.5 h / 1) -10 degC, 2.5 h, 2) room temperature, ca. 45 min 6: benzene-d6 / 2 h / 5 °C / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 8 p. 1262 - 1266
反应条件
trichloromonobromomethane Irradiation;
参考文献
Wang,R.H.S.
Journal of Organic Chemistry, 1972 , vol. 37, p. 2771 - 2774
反应条件
lt;Co(CN)5O2gt;(3-)*3Et4N(1+); oxygen in N,N-dimethyl-formamide T=0°C; 14 h;
参考文献
Nishinaga, A.; Tomita, H.; Matsuura, T.
Tetrahedron Letters, 1980 , vol. 21, p. 2833 - 2836
反应条件
oxygen; thiamine diphosphate in tetrachloromethane Irradiation;
参考文献
Gollnick, Klaus; Schnatterer, Albert
Tetrahedron Letters, 1985 , vol. 26, # 41 p. 5029 - 5032
反应条件
oxygen; cobalt(II)salen in dichloromethane T=20°C; Oxidation; 3 h; Product distribution; Further Variations:Catalysts;
参考文献
Knaudt, Jutta; Foerster, Stefan; Bartsch, Ulrich; Rieker, Anton; Jaeger, Ernst-G.
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 1 p. 86 - 93
反应条件
Co(salN-Medpt) in acetonitrile 24 h; Yield given. Yields of byproduct given;
参考文献
Frostin-Rio, Maryvonne; Pujol, Daniele; Bied-Charreton, Claude; Perree-Fauvet, Martine; Gaudemer, Alain
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 1971 - 1980