4-甲氧基-4-连苯基羧酸乙酯合成路线 （共 49 条）
反应条件
C68H72Cl2N6NiP2; water; lithium chloride; zinc(II) chloride in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=25°C; Kumada coupling reaction; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
pyridine; tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Electrolysisiron rod as anode; stainless steel grid as cathode;
参考文献
Gomes, Paulo; Fillon, Hyacinthe; Gosmini, Corinne; Labbe, Eric; Perichon, Jacques
Tetrahedron, 2002 , vol. 58, # 42 p. 8417 - 8424
反应条件
bis(η3-allyl-μ-chloropalladium(II)); P(C6H4)CH(C(CH3)C(Si(CH3)3))2 in tetrahydrofuran; acetonitrile T=20°C; Negishi coupling reaction; 2 h;
参考文献
Ribagnac, Philippe; Blug, Matthias; Villa-Uribe, Jose; Le Goff, Xavier-Frederic; Gosmini, Corinne; Mezailles, Nicolas
Chemistry - A European Journal, 2011 , vol. 17, # 51 p. 14389 - 14393
反应条件
C27H22Cl2N3NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one 12 h; Inert atmosphereSchlenk techniqueHeating;
参考文献
Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
Dalton Transactions, 2012 , vol. 41, # 34 p. 10453 - 10464,12
反应条件
C27H22Cl2N3NiP in tetrahydrofuran; 1-methyl-pyrrolidin-2-one 3 h; Inert atmosphereSchlenk techniqueHeating;
参考文献
Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
Dalton Transactions, 2012 , vol. 41, # 34 p. 10453 - 10464,12
反应条件
water; triethylamine; Pd(OAc)2EnCatTM in N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura reaction; 0.25 h; microwave irradiation;
参考文献
Synlett, , # 8 p. 1251 - 1254
反应条件
bis(η3-allyl-μ-chloropalladium(II)); caesium carbonate; triphenylphosphine in toluene T=90°C; 12 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Organic Letters, , vol. 5, # 8 p. 1357 - 1360
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C 2.1: TBAF / tetrahydrofuran 2.2: 83 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 9 p. 1495 - 1498
反应条件
1: sulfuric acid / |Reflux 2: palladium diacetate; triphenylphosphine; potassium carbonate / N,N-dimethyl-formamide / |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 22 p. 5738 - 5741
