反应条件
1.1: N,N,N',N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 20 °C / |Inert atmosphere
1.2: 12 h / 20 °C / |Inert atmosphere
2.1: ammonium chloride / water
3.1: palladium diacetate; potassium carbonate; iodine / acetonitrile / 12 h / 20 - 80 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube
View Scheme
参考文献
Niu, Liting; Yang, Haijun; Jiang, Yuyang; Fu, Hua
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3625 - 3632
