(S)-(+)-α-乙酰氧基苯乙酸合成路线 （共 12 条）
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in diethyl ether T=20°C; Acetylation;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 19 p. 3701 - 3718
反应条件
in acetone; toluene T=37°C; 24 h; Pseudomonas sp. lipase;
参考文献
Journal fuer Praktische Chemie/Chemiker-Zeitung, , vol. 334, # 6 p. 526 - 528
参考文献
Tetrahedron, , vol. 59, # 40 p. 8049 - 8056
反应条件
1: With Pseudomonas sp. lipase in di-isopropyl ether T=20°C; 12 h; 2: With mandelate racemase in water T=20°C; pH=7.5; 12 h;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 21 p. 4079 - 4081
反应条件
lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water
参考文献
Tetrahedron Letters, , vol. 49, # 52 p. 7398 - 7402
反应条件
N-isopropylcarbamoyl-derivatized cyclofructan-6 column in ethanol; n-heptane; trifluoroacetic acid T=20°C; Resolution of racemate;
参考文献
Analytical Chemistry, , vol. 81, # 24 p. 10215 - 10226
反应条件
1: 67 percent / H2 / 10percent Pd/C / methanol / 0 °C 2: 77 percent / pyridine / 14 h / 0 - 20 °C 3: 18 percent / ruthenium dioxide, sodium periodate / acetone; H2O / 4.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 10 p. 1904 - 1906
反应条件
ruthenium(IV) oxide; sodium periodate in water; acetone 4.5 h;
参考文献
Journal of Organic Chemistry, , vol. 51, # 10 p. 1904 - 1906
反应条件
1: 77 percent / pyridine / 14 h / 0 - 20 °C 2: 18 percent / ruthenium dioxide, sodium periodate / acetone; H2O / 4.5 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 51, # 10 p. 1904 - 1906
反应条件
recombinant nitrilase from Pseudomonas fluorescens EBC 191 in methanol; phosphate buffer T=25°C; pH=6; 24 h; KineticsProduct distribution; Further Variations:pH-values;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 18 p. 2597 - 2603
