1-甲氧基-2-(甲氧基甲氧基)苯合成路线 （共 14 条）
反应条件
sodium perchlorate in methanol; dichloromethane
anodic oxidation (undivided cell, Pt foil anode, W wire cathode, 50 mA, 3 F mol-1), other substrates; Product distributionMechanism;
参考文献
Pardini, Vera L.; Vargas, Reinaldo R.; Viertler, Hans; Utley, James H. P.
Tetrahedron, 1992 , vol. 48, # 35 p. 7221 - 7228
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rosenberg, Saul H.; Rapoport, Henry
Journal of Organic Chemistry, 1984 , vol. 49, p. 56 - 62
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rosenberg, Saul H.; Rapoport, Henry
Journal of Organic Chemistry, 1984 , vol. 49, p. 56 - 62
反应条件
1.1: n-butyllithium / tetrahydrofuran / 2 h / 20 °C
1.2: 30 percent / iodine / tetrahydrofuran / 2 h / 20 °C
2.1: 94 percent / triphenylphosphine; triethylamine; copper(I) iodide / bis(triphenylphosphine)palladium(II) chloride / 80 °C
3.1: 78 percent / sodium hydroxide / toluene / 3.5 h / Heating
View Scheme
参考文献
Brimble, Margaret A.; Flowers, Christopher L.; Trzoss, Michael; Tsang, Kit Y.
Tetrahedron, 2006 , vol. 62, # 25 p. 5883 - 5896
