2-(1,3-苯并噻唑-2-基氨基)乙硫醇合成路线 (共 2 条)
反应条件
sodium tetrahydroborate in methanol; 2-methoxy-ethanol
T=60°C;
参考文献
Johnston,T.P.; Gallagher,A.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1305 - 1308
反应条件
1: dimethylformamide / 3 h / 70 - 80 °C
2: propan-1-ol / 3.5 h / Heating
3: NaBH4 / methanol; 2-methoxy-ethanol / 60 °C
View Scheme
参考文献
Johnston,T.P.; Gallagher,A.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1305 - 1308