water in diethyl ether
byproducts: H2O; react. of B(OCH3)3 and RMgBr in ether at -75°C, hydrolysis, dehydration of dihydroxy borane (yield:70percent) on boiling with toluene (removal of H2O during course of react.);;
参考文献
Snyder, H. R.; Kuck, J. A.; Johnson, J. R.
Journal of the American Chemical Society, 1938 , vol. 60, p. 105 - 111
Grummitt
Journal of the American Chemical Society, 1942 , vol. 64, p. 1812
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Snyder; Kuck; Johnson
Journal of the American Chemical Society, 1938 , vol. 60, p. 110