反应条件
1: 2.) 1,2-epoxybutane / 1.) CH2Cl2, 2.) acetonitrile, 80 deg C
2: triethylamine / CH2Cl2 / 1 h / 25 °C
3: 75 percent / 10percent HCl / 1,2-dimethoxy-ethane / 6 h / 65 °C
4: 47 percent / triphenylphosphine, diethyl azodicarboxylate / benzene / 65 h / 25 °C
5: Raney nickel / ethanol / 80 °C
6: LiAlH4 / tetrahydrofuran
View Scheme
参考文献
Meyers; Amos
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 870 - 872