2,2-二甲基-1,3-丙二胺合成路线 （共 31 条）
反应条件
hydrogenchloride; water; iron T=100°C; durch Reduktion;
参考文献
Industrial and Engineering Chemistry, , vol. 40, p. 507
反应条件
ethanol; nickel T=60°C; P=51485.6 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3250
US2418237 , ;
反应条件
dimethylsulfide borane complex in tetrahydrofuran 2 h; Heating;
参考文献
Anderson, Wayne K.; Kasliwal, Ravindra; Houston, D. Michael; Wang, Yueh-sha; Narayanan, Ven L.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 19 p. 3789 - 3797
反应条件
silver nitrate in sodium hydroxide; water
反应条件
ammonia; hydrogen; Co-Fe catalyst T=210°C; P=37503 - 112509 Torr; Product distribution;
参考文献
Angewandte Chemie - International Edition, , vol. 38, # 3 p. 351 - 354
反应条件
1: 82 percent / 28percent NH3 2: 75 percent / BH3*SMe2 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 19 p. 3789 - 3797
反应条件
1: 71 percent / SOCl2 / 20 h / Heating 2: 82 percent / 28percent NH3 3: 75 percent / BH3*SMe2 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 19 p. 3789 - 3797
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 36, p. 3042 - 3044
反应条件
1: NaN3 / bis-(2-hydroxy-ethyl) ether / 16 h / 135 °C 2: LiAlH4 / tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 36, p. 3042 - 3044
反应条件
1: pyridine / 24 h / 10 °C 2: NaN3 / bis-(2-hydroxy-ethyl) ether / 16 h / 135 °C 3: LiAlH4 / tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 36, p. 3042 - 3044
