2,2-二甲基-1,3-丙二胺合成路线 （共 31 条）
反应条件
in methanol T=60°C; 24 h;
参考文献
Leung, Man-Kit; Lai, Jun-Liang; Lau, King-Hang; Yu, Hsiao-Hua; Hsiao, Hsiang-Ju
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 4175 - 4179
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4918186 A1, 1990 ;
参考文献
Skinner et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3786
反应条件
in acetonitrile 2 h; Ambient temperature;
参考文献
Kureha Chemical Industry Co., Ltd.
Patent: EP1550657 A1, 2005 ;
Location in patent: Page/Page column 46 ;
反应条件
1: tetrahydrofuran / 14.5 h / 20 °C / Cooling with ice 2: tetrahydrofuran / 15.25 h / 20 °C / Cooling with ice 3: sodium hydroxide; water / methanol / 3 h / 20 - 50 °C View Scheme
参考文献
Jenkins, Thomas E.; Husfeld, Craig O.
Patent: US2012/178772 A1, 2012 ;
参考文献
Skinner; Wunz
Journal of the American Chemical Society, 1951 , vol. 73, p. 3814
反应条件
in diethylene glycol dimethyl ether Reflux;
参考文献
Ihara, Shogo; Soma, Takashi; Yano, Daigo; Aikawa, Shunichi; Yoshida, Yasuhiko
Synthetic Communications, 2011 , vol. 41, # 24 p. 3600 - 3608
反应条件
1: water
2: NaNO3; AgNO3; KOH / acetone; water
View Scheme
参考文献
Kralingen, Cornelis G. van; Reedijk, Jan; Spek, Anthony L.
Inorganic Chemistry, 1980 , vol. 19, p. 1481 - 1485
反应条件
1: water
2: NaNO3; AgNO3 / acetone; water
3: HCl; H2O2 / water
View Scheme
参考文献
Kralingen, Cornelis G. van; Reedijk, Jan; Spek, Anthony L.
Inorganic Chemistry, 1980 , vol. 19, p. 1481 - 1485
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane
Hoffman carbylamine reaction;
参考文献
Al-Ktaifani; Rukiah; Shaaban
Polish Journal of Chemistry, 2008 , vol. 82, # 3 p. 547 - 557
