N-(2-氧代-2-苯基)乙基甲酰胺合成路线 (共 10 条)
反应条件
1: sodium amalgam; alcohol; formic acid / 60 - 70 °C 2: phosphorus pentoxide; toluene View Scheme
参考文献
Chemische Berichte, , vol. 43, p. 2388
反应条件
diphosphorus pentasulfide
参考文献
Bachstez
Chemische Berichte, 1914 , vol. 47, p. 3166
反应条件
potassium hydroxide in ethanol
0.166667 h; Ambient temperature;
参考文献
Yinglin, Han; Hongwen, Hu
Synthesis, 1990 , # 7 p. 615 - 618
反应条件
1: 95 percent / sodium azide / dimethylsulfoxide / 0.5 h / 10 °C
2: 86 percent / HCl, H2 / 10percent Pd/C / methanol / 5 h / 2327.2 Torr / Ambient temperature
3: 86 percent / sodium formate / 1 h / Ambient temperature
View Scheme
参考文献
Ackrell, Jack; Muchowski, Joseph M.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3374 - 3376
反应条件
toluene-4-sulfonic acid
T=140°C; 16 h;
参考文献
LaMattina, John L.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2261 - 2262
反应条件
1: 86 percent / HCl, H2 / 10percent Pd/C / methanol / 5 h / 2327.2 Torr / Ambient temperature
2: 86 percent / sodium formate / 1 h / Ambient temperature
View Scheme
参考文献
Ackrell, Jack; Muchowski, Joseph M.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3374 - 3376
反应条件
in ethanol
2 h; Ambient temperature;
参考文献
Ying-lin, Han; Hong-ven, Hu
Tetrahedron Letters, 1989 , vol. 30, # 39 p. 5285 - 5286
反应条件
sodium formate
1 h; Ambient temperature;
参考文献
Ackrell, Jack; Muchowski, Joseph M.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3374 - 3376
参考文献
Bachstez
Chemische Berichte, 1914 , vol. 47, p. 3166
Show Details
Pictet; Gams
Chemische Berichte, 1910 , vol. 43, p. 2388
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
Heating;
参考文献
Wehrli
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 1915 - 1919