hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; tris(2,4-di-tert-butyl-phenyl) phosphite in toluene T=50°C; 4 h; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 12, # 26 p. 6930 - 6939
1: C57H59O5P2Rh; hydrogen / toluene / 60 h / 45 °C / 22502.3 Torr 2: Cornforth reagent / N,N-dimethyl-formamide; toluene / 20 °C View Scheme
参考文献
Chikkali, Samir H.; Bellini, Rosalba; De Bruin, Bas; Van Der Vlugt, Jarl Ivar; Reek, Joost N. H.
Journal of the American Chemical Society, 2012 , vol. 134, # 15 p. 6607 - 6616