1-叔丁氧羰基-2,3-二氢吡咯合成路线 （共 24 条）
反应条件
1: 87.5 percent / Triethylamine / dioxane; H2O / 15 h / 50 °C
2: 62 percent / Fe(CO)5 / m-xylene / 6 h / 138 °C
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参考文献
Stille, J. K.; Becker Y.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2139 - 2145
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
参考文献
Gomez-Vidal, Jose A.; Silverman, Richard B.
Organic Letters, 2001 , vol. 3, # 16 p. 2481 - 2484
反应条件
1: 88 percent / triethylamine / dioxane; H2O; methanol / 4 h / 20 °C
2: DEAD; PPh3 / tetrahydrofuran
View Scheme
参考文献
Gomez-Vidal, Jose A.; Silverman, Richard B.
Organic Letters, 2001 , vol. 3, # 16 p. 2481 - 2484
反应条件
1: 4-(N,N-dimethlyamino)pyridine / acetonitrile / 3.33 h / 0 °C / |Schlenk technique
2: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.83 h / -78 °C / |Schlenk technique
3: trifluoroacetic anhydride; triethylamine / dichloromethane / 7.25 h / -78 - 20 °C / |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Xie, Yinjun; Hu, Jianhua; Xie, Pan; Qian, Bo; Huang, Hanmin
Journal of the American Chemical Society, 2013 , vol. 135, # 49 p. 18327 - 18330
