反应条件
sulfuric acid in sulfuric acid
byproducts: (CH3)3SiOCH2CH2CH2CH3; addn. of 0.3percent concd. H2SO4 to a mixt. of the borate (0.05 mol) and the silazane (0.1 mol); refluxing for 15 h with continuous Ar flushing;; mixt. not separated, total yield: 48percent;;
参考文献
Svatikov, M. Yu.; Gruzinova, E. A.; Kotrelev, G. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 7.2 p. 1494 - 1496
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 7 p. 1683 - 1685