(4-溴丁基)三苯基溴化膦合成路线 （共 15 条）
反应条件
1: 99 percent / dimethylformamide / 4 h / Heating
2: 98 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 94 percent / dimethylformamide / 4 h / Heating
2: 85 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 99 percent / dimethylformamide / 4 h / Heating
2: 98 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: sulphur / toluene / 2 h
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 94 percent / dimethylformamide / 4 h / Heating
2: 85 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: sulphur / toluene / 2 h
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
sodium amide in ammonia
T=-50°C;
参考文献
Schmidbaur, Hubert; Schier, Annette; Neugebauer, Dietmar
Chemische Berichte, 1983 , vol. 116, # 6 p. 2173 - 2179
