三亚甲基双(三苯基溴化膦)合成路线 (共 5 条)
反应条件
in N,N-dimethyl-formamide
参考文献
Zarbin, Paulo H. G.; Princival, Jefferson L.; De Lima, Eraldo R.; Dos Santos, Alcindo A.; Ambrogio, Bianca G.; De Oliveira, Alfredo R. M.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 239 - 241
参考文献
Balema, Viktor P.; Wiench, Jerzy W.; Pruski, Marek; Pecharsky, Vitalij K.
Chemical Communications, 2002 , # 7 p. 724 - 725
反应条件
potassium carbonate in 1,4-dioxane; water
T=105°C; Wittig reaction; 20 h;
参考文献
Kaltia, Seppo; Matikainen, Jorma; Ala-Peijari, Maija; Hase, Tapio
JAOCS, Journal of the American Oil Chemists' Society, 2008 , vol. 85, # 6 p. 561 - 565
反应条件
lithium diisopropyl amide in tetrahydrofuran
Elimination;
参考文献
Pohnert, Georg; Boland, Wilhelm
European Journal of Organic Chemistry, 2000 , # 9 p. 1821 - 1826
反应条件
sodium hexamethyldisilazane in diethyl ether
3 h; Ambient temperature; Yields of byproduct given;
参考文献
Bestmann; Zeibig; Vostrowsky
Synthesis, 1990 , # 11 p. 1039 - 1047