1: allyltriphenylsilane With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: p-EtOC(O)C6H4Cl With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 5 h;
1: PTAS With tetrabutyl ammonium fluoride in tetrahydrofuran; water T=20°C; 1 h; 2: p-EtOC(O)C6H4Cl With 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran; water T=80°C; 4 h;
1: phenyl-magnesium chloride With titanium tetraethoxide in tetrahydrofuran T=0°C; 2: p-EtOC(O)C6H4Cl With 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=25°C; 24 h; Further stages.;
参考文献
Manolikakes, Georg; Dastbaravardeh, Navid; Knochel, Paul
Synlett, 2007 , # 13 p. 2077 - 2080
