1-羟基-4-甲氧基蒽醌合成路线 （共 34 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Russell, Richard A.; Warrener, Ronald N.
Journal of the Chemical Society, Chemical Communications, 1981 , # 3 p. 108 - 110
反应条件
potassium hydroxide
T=100°C;
参考文献
Eckert; Steiner
Monatshefte fuer Chemie, 1914 , vol. 35, p. 1154
反应条件
1: 170 mg / CH2Cl2 / 72 h
2: 2.7 mg / 5percent aq. H2SO4, acetic acid / 0.25 h / Heating
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; McKay, Peter G.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2095 - 2109
反应条件
1: 170 mg / CH2Cl2 / 72 h
2: 2.7 mg / 5percent aq. H2SO4, acetic acid / 0.25 h / Heating
View Scheme
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; McKay, Peter G.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2095 - 2109
反应条件
1: 85 percent / sodium methoxide / methanol / 0.08 h / -20 °C
2: 76 percent / 3,5-dimethylpyrazole, chromium trioxide / CH2Cl2 / 5 h / Heating
View Scheme
参考文献
Russell, Richard A.; Evans, David A. C.; Warrener, Ronald N.
Australian Journal of Chemistry, 1984 , vol. 37, # 8 p. 1699 - 1707
反应条件
1: 83 percent / bromine / CHCl3 / 1 h
2: 61 percent / potassium hydroxide / H2O / 2 h / Heating
3: 1.) lithium di-isopropylamide, 2.) air / 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h
View Scheme
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
反应条件
1: 1.) n-butyl-lithium / 1.) ether, hexane, reflux, 24 h, 2.) - 78 deg C -> ambient temperature
2: 1.) lithium di-isopropylamide, 2.) air / 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h
View Scheme
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
反应条件
perchloric acid
12 h; Heating;
参考文献
Carretero, Juan Carlos; Cuevas, Juan Carlos; Echavarren, Antonio; Prados, Pilar; Farina, Francisco
Journal of Chemical Research, Miniprint, 1984 , # 1 p. 147 - 194
反应条件
silver(l) oxide in chloroform
参考文献
Cameron, Donald W.; Feutrill, Geoffrey I.; McKay, Peter G.
Australian Journal of Chemistry, 1982 , vol. 35, # 10 p. 2095 - 2109
反应条件
1: 1.) lithium di-isopropylamide, 2.) air / 1.) THF, -70 - -60 deg C, 2.) THF, 20 deg C, 22 h
2: 98 percent / conc. hydrochloric acid / tetrahydrofuran / 15 h / Ambient temperature
View Scheme
参考文献
Dodsworth, David J.; Calcagno, Maria-Pia; Ehrmann, E. Ursula; Devadas, Bhatt; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2120 - 2124
