二(正丁基环戊二烯基)二氯化锆(IV)合成路线 （共 2 条）
反应条件
n-butyllithium in tetrahydrofuran; ethylene glycol dimethyl ether; hexane 1:1 mixt. of 1- and 2-(n-C4H9)C5H5 was dissolved in THF and treated with n-BuLi in hexane followed by ZrCl4 in glyme; recrystd. from heptane; elem. anal.;
参考文献
Newmark, Richard A.; Boardman, Larry D.; Siedle, Allen R.
Inorganic Chemistry, 1991 , vol. 30, p. 853 - 856
反应条件
in toluene T=20°C; 20 h; Heating / reflux;
参考文献
Chevron Phillips Chemical Company, L.P.
Patent: US2008/4460 A1, 2008 ;
Location in patent: Page/Page column 24-25 ;
