反应条件
1: 41 percent / CH3COOK / methanol / 10 h / Heating
2: 51 percent / diethyl ether / 0.25 h / 0 °C / 5 recycles
3: 28 percent / Potassium hydride / hexamethylphosphoric acid triamide; tetrahydrofuran / 2 h / Ambient temperature
4: 41 percent / KOH, hydrazine hydrate (85percent) / various solvent(s) / 6 h / Heating
5: 72 percent / HgO, BF3-OEt2 / tetrahydrofuran; H2O / 1.5 h / Ambient temperature
View Scheme
参考文献
Wilson, Stephen R.; Misra, Raj N.; Georgiadis, Gregory M.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2460 - 2468