4-(乙基氨基甲基)-3,4-二氢-2H-噻喃并[2,3-b]吲哚-9-甲醛盐酸盐合成路线 （共 2 条）
反应条件
1: 93 percent / Et3N / tetrahydrofuran / 1 h / Ambient temperature
2: 1) 50 percent NaH / 1.) oil, DMF, RT, 1 h; 2.) DMF, oil, RT, 1.5 h
3: 1) CF3COOH; 2) HCl / CH2Cl2 / 2 h
View Scheme
参考文献
Takada; Ishizuka; Sasatani; Makisumi; Jyoyama; Hatakeyama; Asanuma; Hirose
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 3 p. 877 - 886
反应条件
1: 1) 50 percent NaH / 1.) oil, DMF, RT, 1 h; 2.) DMF, oil, RT, 1.5 h
2: 1) CF3COOH; 2) HCl / CH2Cl2 / 2 h
View Scheme
参考文献
Takada; Ishizuka; Sasatani; Makisumi; Jyoyama; Hatakeyama; Asanuma; Hirose
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 3 p. 877 - 886
