in diethyl ether byproducts: LiCl; reaction mixture cooled to -50°C; stirred for 2 h at room temp.;; filtered; ether was removed under vacuum; distilled at 50°C at 0.2 Torr;;
参考文献
Wan, Yanjian; Verkade, John G.
Inorganic Chemistry, 1993 , vol. 32, p. 79 - 81
in tetrahydrofuran byproducts: LiOSi(CH3)3; a suspn. of germatrane in THF was treated with an excess of (Me2)NLi inn-hexane at room temp. for 4 h; evap., filtered;
参考文献
Karlov, Sergey S.; Shutov, Pavel L.; Akhmedov, Novruz G.; Seip, Markus A.; Lorberth, Joerg; Zaitseva, Galina S.
Journal of Organometallic Chemistry, 2000 , vol. 598, # 2 p. 387 - 394
