反应条件
1: 80 percent / TMEDA, n-BuLi / hexane; tetrahydrofuran / 1.) -78 deg C to -20 deg C, 2 h, 2.) room temperature, overnight
2: 1.) NBS, benzoylperoxide, 2.) AlCl3 / 1.) CCl4, irradiation, reflux, overnight, 2.) CH3NO2, room temperature, 1 h
View Scheme
参考文献
Sartori; Bigi; Tao; Porta; Maggi; Predieri; Lanfranchi; Pellinghelli
Journal of Organic Chemistry, 1995 , vol. 60, # 20 p. 6588 - 6591
