N,N-二异丙基-对甲苯胺合成路线 (共 8 条)
反应条件
C22H26Cl2NPPd; sodium t-butanolate in toluene
T=110°C; 22 h; Inert atmosphere;
参考文献
Samblanet, Danielle C.; Schmidt, Joseph A. R.
Journal of Organometallic Chemistry, 2012 , vol. 720, p. 7 - 18,12
反应条件
n-butyllithium
T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wickham, Peter P.; Hazen, Kevin H.; Guo, Hong; Jones, Garth; Reuter, Kelly Hardee; Scott, William J.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2045 - 2050
反应条件
n-butyllithium
T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wickham, Peter P.; Hazen, Kevin H.; Guo, Hong; Jones, Garth; Reuter, Kelly Hardee; Scott, William J.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2045 - 2050
反应条件
1: dipotassium hydrogenphosphate; N,N-dimethyl-formamide / 25 °C / Inert atmosphere
2: toluene / 1 h / 25 °C / Inert atmosphere
View Scheme
参考文献
Rucker, Richard P.; Whittaker, Aaron M.; Dang, Hester; Lalic, Gojko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 16 p. 3953 - 3956
反应条件
in toluene
T=25°C; 1 h; Inert atmosphere;
参考文献
Rucker, Richard P.; Whittaker, Aaron M.; Dang, Hester; Lalic, Gojko
Angewandte Chemie - International Edition, 2012 , vol. 51, # 16 p. 3953 - 3956
参考文献
Bacchetti; Ferrati
Gazzetta Chimica Italiana, 1956 , vol. 86, p. 722,725
反应条件
1: ethanol
2: Raney nickel
View Scheme
参考文献
Bacchetti; Ferrati
Gazzetta Chimica Italiana, 1956 , vol. 86, p. 722,725
反应条件
1: ethanol
2: Raney nickel
View Scheme
参考文献
Bacchetti; Ferrati
Gazzetta Chimica Italiana, 1956 , vol. 86, p. 722,725